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The fractured surface of the specimen is coated with a heavy metal layer with the metal

being deposited at an angle. A uniform carbon layer is deposited on top of the metal layer from directly
overhead to cement the patches of metal into a solid layer. What is the name for this process?
A) freeze-fracture
B) replication
C) entrapment
D) metallification
E) freeze-etch

1 Answer

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Final answer:

The process is called freeze-etching, a sample preparation method for SEM imaging, where metal and carbon layers are deposited to visualize specimen surfaces.

Step-by-step explanation:

The process described in the question is known as freeze-etching or freeze-etching. In this process, samples are prepared for examination, usually through a Scanning Electron Microscope (SEM). A sample is first fractured, often at cryogenic temperatures, to reveal its internal structures. Then, a heavy metal layer is deposited at an angle to shadow the exposed surfaces, providing contrast and highlighting topographical features.

Next, a uniform carbon layer is deposited from above to create a solid layer that cements the metal patches, preserving the three-dimensional structure of the specimen. This prepares the sample for electron microscopy by making it conductive and preventing charging under the electron beam, thus allowing for high-resolution imaging of surfaces and structures.

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