Answer:
Hence,
1) removed
2) drained through the stopcock
3) get eye level with
4) slow the draining
5) switch to a new flask
Step-by-step explanation:
After mixing the solutions in a separatory funnel, the stopper should be removed and the liquid should be drained through the stopcock, and the layers allowed to separate. When you get close to the interface between the layers, get eye level with the funnel and turn over to slow the draining heat up until the first layer is collected. Switch to a new flask get eye level with it to collect the second layer.