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If the solubility of salicylic acid is 77.8 g/L of water at 100oC and 1.4 g/L of water at 10oC, a) calculate the minimum amount (in mL) of boiling water necessary to dissolve 2.0 g of impure salicylic acid for recrystallization. b) If the solution is cooled to room temperature and then to 10oC with an ice/water bath, what is the maximum amount of solid salicylic acid isolated after vacuum filtration

User Shrhawk
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2 Answers

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21 votes

Final answer:

To dissolve 2.0 g of impure salicylic acid for recrystallization, approximately 0.19 mL of boiling water is needed. After cooling, the maximum amount of solid salicylic acid isolated after vacuum filtration is approximately 1430 mL.

Step-by-step explanation:

To calculate the minimum amount of boiling water necessary to dissolve 2.0 g of impure salicylic acid for recrystallization, you need to convert the mass of salicylic acid into moles using its molar mass. Then, you can use the solubility data to determine the volume of boiling water needed. The molar mass of salicylic acid is 138.1 g/mol, so 2.0 g is equivalent to 2.0/138.1 = 0.0145 mol. Using the solubility at 100°C, 77.8 g/L, you can calculate the volume of boiling water needed as 0.0145 mol / (77.8 g/L) = 0.00019 L or 0.19 mL.

When the solution is cooled to room temperature and then to 10°C with an ice/water bath, the solubility of salicylic acid decreases. According to the solubility data, at 10°C the solubility is 1.4 g/L. To determine the maximum amount of solid salicylic acid isolated after vacuum filtration, you need to calculate the volume of water that can hold 2.0 g of salicylic acid at 10°C. Using the solubility at 10°C of 1.4 g/L, you can calculate the maximum volume of water as 2.0 g / (1.4 g/L) = 1.43 L or 1430 mL.

User Nikravi
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16 votes
16 votes

Answer:

a. 25.7mL are necessaries.

b. 1.964g of salicylic acid can be isolated.

Step-by-step explanation:

a. As the solubility of salicylicic acid in boiling water is 77.8g/L, to dissolve 2.0g of salicylic acid are necessaries:

2.0g * (1L / 77.8g) = 0.0257L =

25.7mL are necessaries

b. Then, at 10°C the solution just can dissolve 1.4g/L, that is:

0.0257L * (1.4g/L) = 0.036g of salicylic acid are dissolved.

And will precipitate:

2.0g - 0.036g =

1.964g of salicylic acid can be isolated

User Jarin Rocks
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