Final answer:
The volume increase in the experiment is due to the formation of carbon dioxide gas.
Step-by-step explanation:
The volume increase in the experiment is due to the formation of carbon dioxide gas (b). When calcium carbonate reacts with hydrochloric acid, one of the products formed is carbon dioxide gas. This gas occupies space and increases the overall volume of the system. The reaction can be represented by the equation: CaCO3(s) + 2HCl(aq) → CaCl2(aq) + CO2(g) + H2O(l).