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0.6g of organic compound on Kjeldahl's analysis produced ammonia, which is absorbed in 90 ml of N/9 H2SO4. The excess acid left requires 20 ml of N/10 of NaOH for complete neutralization. Calculate the percentage of nitrogen in the organic.

(a) 7.2%
(b) 9.6%
(c) 11.2%
(d) 13.8%

User RyanL
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1 Answer

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Final answer:

By using Kjeldahl's method, the percentage of nitrogen in the organic compound is calculated to be 19.07%, which does not match the given answer choices, suggesting a possible typo or error.

Step-by-step explanation:

The student is asking to calculate the percentage of nitrogen in an organic compound by using Kjeldahl's method. Initially, 0.6g of the compound produced ammonia, which required 90 ml of N/9 H2SO4 for absorption. Since there was excess acid, it took 20 ml of N/10 NaOH to neutralize it. To find the amount of acid neutralized by the ammonia, we subtract the amount of NaOH used from the amount of H2SO4 added:

  • 90 ml of N/9 H2SO4 = 10 ml of N H2SO4
  • 20 ml of N/10 NaOH = 2 ml of N NaOH
  • So, the ammonia has neutralized 10 ml - 2 ml = 8 ml of N H2SO4.

Since the reaction between H2SO4 and NH3 is 1:2, the moles of NH3 are double the moles of H2SO4 neutralized. Therefore:

  • 8 ml of N H2SO4 = 8/1000 moles = 8 x 10^-3 moles of H2SO4
  • Which means 16 x 10^-3 moles of NH3
  • Since the molar mass of NH3 is 17 g/mol, the mass of NH3 from the 0.6 g sample is 16 x 10^-3 moles x 17 g/mol = 0.272 g NH3, which contains 82 x 10^-3 moles x 14 g/mol = 0.1144 g of N

Lastly, to find the percentage of nitrogen:

  • (0.1144 g / 0.6 g) x 100 = 19.07%

However, none of the given answer choices match this correct result, indicating that there may have been a typo in the question options or a misinterpretation during the process.

User Regnauld
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