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1) A student is performing the scparation of benroic acid from acetanilide. The student recowers 4.24 grams of berzoic acid and 9.25 grams acetanilide. Assuming that more than 95% of the material was recovered; what is the % composition of the original mixture?

2) What incorrect conclusion would be made about a sample whose melting point was recorded using a temperature ramp greater than 5 ∘C per minute?
3) What family of organic compounds does trimyristin belong to? 13) Explain the purpose of adding Calcium Carbonate to the tea solution before extracting with methylene chloride.
4) Explain the purpose of using a melting point standard alongside any melting point sample.
5) The melting point of pure caffeine is 236 ∘C. Why would the observed melting point of a pure caffeine sample be considerably lower?

1 Answer

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Final answer:

To calculate the molar mass of the solution, use the formula Moles of solute = Mass of solute / Molar mass of solute. The incorrect conclusion made about a sample with a melting point recorded using a temperature ramp greater than 5 ∘C per minute is that the sample has a lower melting point than it actually does. Trimyristin belongs to the family of organic compounds called triglycerides. Adding Calcium Carbonate to the tea solution before extracting with methylene chloride helps neutralize acidic compounds. Using a melting point standard alongside a melting point sample verifies the measurement's accuracy. The observed melting point of a pure caffeine sample may be considerably lower due to impurities.

Step-by-step explanation:

The molar mass of a solution can be calculated using the formula:

Moles of solute = Mass of solute / Molar mass of solute

In this case, the mass of the compound is 5.00 g and the mass of carbon tetrachloride is 25.00 g. The boiling point elevation constant (K₁) for carbon tetrachloride is 5.02 °C/m.

To calculate the molar mass of the compound, we need to find the change in boiling point (ΔT) and the molality of the solution (m).

ΔT = K₁ × m

m = Molality of solution = Moles of solute / Mass of solvent (in kg)

Using the given data, we can calculate the molar mass of the compound.

The incorrect conclusion that would be made about a sample whose melting point was recorded using a temperature ramp greater than 5 ∘C per minute is that the sample has a lower melting point than it actually does. A higher temperature ramp rate can cause a sample to heat up and melt faster, suggesting a lower melting point.

Trimyristin belongs to the family of organic compounds called triglycerides, which are esters derived from glycerol and three fatty acids. It is commonly found in the oil extracted from nutmeg.

The purpose of adding Calcium Carbonate to the tea solution before extracting with methylene chloride is to neutralize any acidic compounds present in the tea. Calcium Carbonate acts as a base, reacting with acids to form a salt and water. This helps to remove any acidic impurities from the tea solution before further extraction.

The purpose of using a melting point standard alongside any melting point sample is to verify the accuracy and precision of the melting point measurement. The melting point standard is a compound with a known and well-defined melting point. By comparing the melting point of the sample with that of the standard, we can ensure that the measurement is reliable.

The observed melting point of a pure caffeine sample may be considerably lower due to impurities present in the sample. Impurities can lower the melting point of a substance by disrupting the regular arrangement of molecules in the crystal lattice. These impurities can include other compounds, moisture, or even manufacturing residues.

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