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What is an experiment that can verify that new substances are formed and heat is released or absorbed during a chemcal reaction?

What is an experiment that can verify that new substances are formed and heat is released or absorbed during a chemcal reaction?
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What is an experiment that can verify that new substances are formed and heat is released or absorbed during a chemcal reaction?

User OpenSorceress
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An exothermic reactions experiment and endothermic reactions experiment. 
User DataFramed
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