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Write down a specific step by step procedure of the titration process which the goal is to determine the unknown concentration of a basic solution.

User Sartaj Singh Gill
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1 Answer

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21 votes

Step-by-step explanation:

Titration is a technique used to determine the amount of matter in a sample using a solution of known concentration. In other words, titration is a quantitative chemical analysis. In this process, the sample has its concentration determined through a chemical reaction when it is mixed with another substance. The use of pH indicators in this process is useful to determine the endpoint of the titration, indicating that the entire sample has reacted. Titration is used to accurately determine the amount of a substance, confirm that the concentration described on the label is true or that the amount of a chemical compound is indicated on the package.

Sample weighing: With the solid sample on a watch glass, weigh it on the balance.

Sample dissolution: The sample is transferred to an Erlenmeyer flask with water, where dissolution takes place.

Problem solution: The solution is transferred to a volumetric flask and the volume is made up with water, creating the problem solution.

Aliquot transfer: Remove an aliquot of the problem solution with the aid of a pipette and transfer it to an Erlenmeyer flask.

Titration: To the Erlenmeyer flask, the problem solution (titrated) is added and the solution of known concentration (titrant) is inserted into the burette.

An acid-base indicator is also added to the titrator to indicate when the titration should be stopped due to the color change. The color change indicates the end point or turning point of the titration.

After that, when the color change persists, the volume of titrant used is verified and stoichiometric calculations will help us to discover the concentration of the titrated solution.

Answer:

Step 1 - Sample weighing: With the solid sample on a watch glass, weigh it on the balance.

Step 2 - Sample dissolution: The sample is transferred to an Erlenmeyer flask with water, where dissolution takes place.

Step 3 - Problem solution: The solution is transferred to a volumetric flask and the volume is made up with water, creating the problem solution.

Step 4 - Aliquot transfer: Remove an aliquot of the problem solution with the aid of a pipette and transfer it to an Erlenmeyer flask.

Step 5 - Titration: To the Erlenmeyer flask, the problem solution (titrated - basic solution) is added and the solution of known concentration (titrant - acidic solution) is inserted into the burette.

Step 6 - An acid-base indicator is also added to the titrator to indicate when the titration should be stopped due to the color change. The color change indicates the endpoint or turning point of the titration.

Step 7 - After that, when the color change persists, the volume of titrant used is verified and stoichiometric calculations will help us to discover the concentration of the titrated solution.

User Madmaze
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