Final answer:
To extract 3-nitroaniline, use dichloromethane. To extract aniline, use 5% HCl. To extract benzoic acid, use 6 M NaOH.
Step-by-step explanation:
To extract reconstituted 3-nitroaniline out of the aqueous solution, you would use a nonpolar organic solvent such as dichloromethane.
To extract aniline into the aqueous layer, you would use a 5% HCl solution. Aniline is basic and reacts with the acidic environment to form anilinium ion, which is water-soluble.
To extract benzoic acid into the aqueous layer, you would use a 6 M NaOH solution. Benzoic acid reacts with the basic environment to form its water-soluble sodium salt, sodium benzoate.