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What is wrong with this experiment? "when it was heated, the sample of carbon decomposed?"?

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The statement is wrong because carbon does not decompose in the presence of heat. Since carbon contains a large potential energy translated to its calorific value, it is a combustible matter. Thus, in the presence of heat, it gets combusted, or in simple words, it will be burned. As a result, it will yield products in the form of carbon dioxide and water. 
User Anton Kovalenko
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